LARISSA OLIVEIRA BERBEL

LARISSA OLIVEIRA BERBEL

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The corrosion behavior on AA2050-T84 and AA7050-T7451 welded and non-welded by FSW
2021 - VIVEIROS, BARBARA V.G. de; BERBEL, LARISSA O.; DONATUS, UYIME; COSTA, ISOLDA
In this work, the corrosion resistance of the AA2050-T84 and AA7050-T7451 alloys welded by FSW and non-welded was investigated using chloride solutions. The corrosion resistance, microstructure and microhardness were studied. Microhardness measurements at the cross section and at the top surface of the weld identified significant differences between the various zones resulting from FSW. Characterization of the corrosion resistance was carried out by electrochemical and immersion tests. Localized electrochemical techniques were used in this work, specifically scanning vibrating electrode technique (SVET) and scanning ion-selective electrode technique (SIET). The results showed that the most electrochemically active zone at of the welded alloys was the thermomechanically affected zone (TMAZ). This zone corresponds to the transition between the two alloys. In the top surface of the welded alloys, besides the TMAZ, the heat affected zone (HAZ) was also highly active corresponding to the transition between zones of the AA7050. This was due to the formation of hardening precipitates in the HAZ of the AA7050. In the cross-section, the high activity related to the TMAZ was due to the galvanic coupling between the two alloys where the AA7050 alloy acted as anodic zones, and the AA2050, as the cathodic ones. When the two alloys, AA2050 and AA7050, were exposed separately to 0.005 mol.L-1 NaCl or 3.5 (wt%) NaCl solutions, the AA2050 alloy showed higher electrochemical activity compared to the AA7050 alloy which was due to the higher content of active micrometric precipitates in the AA2050 alloy relatively to the AA7050. However, when the alloys were coupled, the AA2050 was cathodically protected by the AA7050 alloy.
Comparing the corrosion behaviour of AA2050 and AA7050 aluminium alloys by scanning vibrating electrode and scanning ion-selective electrode techniques
2022 - VIVEIROS, BARBARA V.G. de; DONATUS, UYIME; ALENCAR, MAICON C. de; BERBEL, LARISSA O.; COSTA, ISOLDA
The susceptibility to localised corrosion of the high strength alloys, AA2050-T84 and AA7050-T7451, used in the aerospace industry, was investigated in this study by localised electrochemical techniques, specifically, scanning vibrating electrode technique (SVET) and scanning ion-selective electrode technique (SIET), in 0.005 mol L−1 NaCl solution. The study was initially carried out using both alloys individually and then, coupling the two alloys and evaluating the effect of galvanic coupling between them. The results revealed that the AA2050-T84, being nobler than the AA7050-T7451, presented higher corrosion current density values when tested in isolation and the depth of corrosion penetration was significantly deeper in the AA2050-T84 alloy than in the AA7050-T7451. However, galvanic coupling of the two alloys resulted in cathodic protection of the AA2050-T84 alloy and a reduction in corrosion current densities on both alloys.
The corrosion resistance between AA2050-T84 and AA7050-T7451 welded by friction stir weld
2019 - VIVEIROS, BARBARA V.G. de; BERBEL, LARISSA O.; BUGARIN, ALINE F.S.; DONATUS, UYIME; COSTA, ISOLDA
Aluminum alloys of the 2XXX and 7XXX series are among the most used materials in the aerospace industry. These alloys have good mechanical, specific strength and corrosion resistance, and for the 2XXX series, further reduction in density can be achieved by lithium addition. So, in this case, it can reduce the weight of the aeroplane and fuel usage leading to the minimization of CO 2 emissions and cost savings. Aluminum alloys have poor weldability, and to use these alloys for aeroplane structures, joining is unavoidable. To make this, the industry uses rivets to join these alloys. But rivets increase the mass of aeroplanes, and to minimise this, a non-fusion (unconventional) welding technique capable of welding aluminium alloys easily was developed. This new technique is friction stir welding, which exposes the aluminum alloys to thermomechanical effects, changing the microstructure of the alloys, and resulting in different regions with different metallurgical and mechanical properties. An example of the regions is the thermomechanically affected region which experiences both plastic deformation and high temperature but without recrystallization. There is also the stir zone which is the region of recrystallized grains, the heat affected zone and the base metal (that is not affected by the welding process). The goals of this work are to analyze the corrosion resistance of the friction stir weldment of dissimilar AA2050-T84 and AA7050-T7451 alloys using electrochemical tests, characterizing the different regions of the weldment, and establishing the most susceptible region to corrosion using a sodium chloride solution.
Estudo da resistência à corrosão das ligas AA2050-T84 e AA7050-T7451 soldadas por FSW
2018 - VIVEIROS, B.V.G. de; ALENCAR, M.C.; BERBEL, L.O.; DONATUS, U.; COSTA, I.
As ligas de alumínio da série 2XXX e 7XXX são muito utilizadas comercialmente em indústrias aeronáuticas pela presença de boas características como resistência à corrosão, resistência mecânica e baixa densidade. Porém, quando soldadas, suas microestruturas sofrem mudanças, o que altera suas propriedades. Neste estudo, as ligas 2XXX e 7XXX foram soldadas pelo método de fricção e mistura, também conhecido como “friction stir welding” (FSW), que aquece e quebra os grãos pela tensão aplicada resultando na soldagem no estado sólido das duas ligas. Neste estudo a resistência à corrosão das ligas AA2050-T84 e AA7050-T7451 soldadas por FSW foi investigada pela técnica “Scanning Vibrating Electrode Technique” (SVET), e por “Scanning Ion - Electrode Technique” (SIET), em que foi realizada a medição de pH localizado. O eletrólito usado neste estudo foi composto por 5 mM de NaCl sendo que a região analisada da solda foi a secção transversal. As zonas afetadas pelo processo FSW são apresentadas e caracterizadas a partir do tamanho de grãos existentes, como metal base (MB), zona termicamente afetada (ZTA), zona termomecanicamente afetada (ZTMA), zona de transição da zona termomecanicamente afetada das ligas (ZTMA trans) e a zona de mistura (ZM), que é a área de recristalização dos grãos. Foram também realizados ensaios de potencial de circuito aberto (OCP) e impedância eletroquímica (EIS) nas mesmas regiões observadas e ensaiadas dos ensaios anteriores, também com solução de 5 mM de NaCl. Os resultados mostraram que nas primeiras horas de ensaio, a área mais suscetível ao ataque foi a zona de transição das ligas (ZTMA trans), mas após 24 h de ensaio, a zona mais suscetível foi a ZTMA da liga 7050-T7451. Esses resultados foram correlacionados com a microestrutura das diferentes zonas.
Qualitative use of potentiodynamic polarization and anodic hydrogen evolution in the assessment of corrosion susceptibility in AA2198-T851 Al–Cu–Li alloy
2018 - DONATUS, UYIME; BERBEL, LARISSA O.; COSTA, ISOLDA
In this study, the corrosion behavior of the AA2198-T851 and its friction stir weldment was used to show the qualitative use of potentiodynamic polarization and the effect of anodic hydrogen evolution (AHE). The results showed that some details can be revealed in the anodic arm of the polarization curves of an Al alloy above the breakdown potential with changes in cell configuration and electrolytes. In addition, AHEinterferes with the measured current density in the anodic arm, which in turn can be used to assess the extent of corrosion susceptibility and changes in anodic dissolution behavior of the alloy.