CAMILA NEVES LANGE
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Artigo IPEN-doc 25077 Stability assessment of a bovine kidney reference-material candidate2018 - CASTRO, LILIANA; MOREIRA, EDSON G.; VASCONCELLOS, MARINA B.A.; LANGE, CAMILA N.; PEDRON, TATIANA; BATISTA, BRUNO L.Reference materials are used worldwide and necessary for quality control purposes during analytical determinations. The present study describes the stability evaluation of a bovine kidney reference-material candidate. An isochronous layout was performed, in which the flasks involved are exposed at different temperatures for different time periods and then are analyzed at the same time at the end of the study. The mass fractions of ten inorganic constituents were determined using instrumental neutron activation analysis and inductively coupled plasma mass spectrometry. Statistical analysis, univariate and multivariate, showed no significant differences in composition between units exposed to the different temperatures and times. The reference material may be transported under normal transportation conditions and the certified values and uncertainties will continue to be valid for a period of 2 years.Artigo IPEN-doc 24747 Potentially toxic elements downward mobility in an impounded vehicle scrapyard2018 - LANGE, CAMILA N.; FIGUEIREDO, ANA M.G.; ENZWEILER, JACINTA; MONTEIRO, LUCILENA R.In Brazil impounded vehicle scrapyards (IVS) are often overcrowded and may pose a source of potentially toxic elements (PTEs). In this study, PTEs content in soil cores and groundwater of an IVS located at a municipality of the So Paulo metropolitan region was assessed. INAA, XRF and ICP-MS were the analytical techniques employed. PTEs results and statistical approaches indicated that As, Pb, Ni, Cu and Nb are mostly anthropic. Pb, Cu, Ni and Nb mass fraction increased with depth indicating some downward mobility. Arsenic may represent a moderate to very high potential ecological risk. PTEs groundwater levels were bellow drinking water recommendation limits.Artigo IPEN-doc 24116 Determinação de impurezas inorgânicas em henna para sobrancelhas para aplicação cosmética2017 - MARINHEIRO, THAMIRES S.; LANGE, CAMILA N.; FIGUEIREDO, ANA M.G.; TICIANELLI, REGINA B.; JESUS, TATIANE A. deAlguns cosméticos podem conter impurezas inorgânicas que, dependendo do nível de fração em massa das mesmas na composição do produto, podem causar efeitos nocivos à saúde humana. A henna (Lawsonia inermis) é uma planta, e o pó, obtido de suas folhas secas e maceradas, é comercializado para coloração de cabelos e sobrancelhas. É comum o uso de henna como alternativa às colorações sintéticas, especialmente para os consumidores que preferem produtos cosméticos naturais ou orgânicos, pois estes são tidos como seguros. Entretanto, algumas hennas comerciais são dopadas com materiais que intensificam a cor e diminuem o tempo de aplicação do produto, estes podem ser de origem mineral ou sais iônicos. Estudos do conteúdo de elementos inorgânicos em hennas comercializadas no Brasil são escassos, apesar de o Brasil ser um dos maiores mercados consumidores de cosméticos do mundo e a aplicação de hennas em sobrancelhas ter aumentado nos últimos anos. O objetivo deste estudo foi avaliar a fração em massa de Ba, Cd, Co, Cr, Fe, Ni e Zn em hennas para coloração de sobrancelhas. Hennas de diferentes cores e marcas comercializadas no mercado e aplicadas em salões de cabelereiro foram analisadas. Quatro das 11 amostras analisadas apresentaram valores de fração em massa de bário cerca de 250 vezes maior que o valor preconizado pela agência nacional de vigilância sanitária (ANVISA), fato que pode representar um potencial risco aos usuários deste tipo de produto. As frações em massa de Cd, Co, Cr, Fe, Ni e Zn apresentaram valores abaixo dos limites regulamentados para cosméticos.Artigo IPEN-doc 22834 Trace elements status in the terrain of an impounded vehicle scrapyard2017 - LANGE, CAMILA N.; FIGUEIREDO, ANA M.G.; ENZWEILER, JACINTA; CASTRO, LILIANAThe impact of a scrapyard of impounded vehicles in Sa˜o Paulo state on topsoil was evaluated for As, Ba, Co, Cr, Cu, Mo, Ni, Pb, V, Zn and rare earth elements (REEs). Mass fractions of all elements, except for Co, Cu, Mo and Zn, were higher than reference values. Hot spots were observed for most elements suggesting vehicular source. The geoaccumulation index showed moderate pollution of As. The enrichment factor pointed to a significant enrichment of As, Mo and Pb. The normalization of REEs to Earth’s crust values indicated a positive anomaly of Ce. The results indicate a potential risk to the soil quality of the scrapyard.Artigo IPEN-doc 22766 A Brazilian coal fly ash as a potential source of rare earth elements2017 - LANGE, CAMILA N.; CAMARGO, IARA M.C.; FIGUEIREDO, ANA MARIA G.M.; CASTRO, LILIANA; VASCONCELLOS, MARINA B.A.; TICIANELLI, REGINA B.Rare earth elements (REEs) have several applications and their market demands have increased. Recently, coal fly ash (CFA) has been considered as a source of these elements. The purpose of this study was to evaluate the REEs content in a CFA from a Brazilian coal power plant by instrumental neutron analysis, to classify it according to commercial purposes and to assess the weathering impact in the REEs content, since it is held in fields nearby the power plant. The results pointed no significant REEs leachability and indicated this CFA as a promising REEs source.Resumo IPEN-doc 22493 Rare earth elements content and leachability in coal fly ash from figueira coal power plant2016 - LANGE, CAMILA N.; VASCONCELLOS, MARINA B.A.; FIGUEIREDO, ANA M.G.; CAMARGO, IARA M.C. de; CASTRO, LILIANA; TICIANELLI, REGINA B.Artigo IPEN-doc 21161 Uncertainty analysis in comparative NAA applied to geological and biological matrices2015 - ZAHN, GUILHERME S.; TICIANELLI, REGINA B.; LANGE, CAMILA N.; FAVARO, DEBORAH I.T.; FIGUEIREDO, ANA M.G.Artigo IPEN-doc 20993 Evaluation of Co and Cr mobility in soil profile collected in a scrapyard of impounded vehicles2015 - LANGE, CAMILA N.; FIGUEIREDO, ANA M.G.; ENZWEILER, JACINTA