ANGEL VISENTIM ORTIZ
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Capítulo IPEN-doc 25004 Mechanical, thermal, morphology and barrier properties of flexible film based on polyethylene-ethylene vinyl alcohol blend reinforced with graphene oxide2017 - SANTANA, JULYANA G.; ORTIZ, ANGEL; OLIVEIRA, RENE R.; RANGARI, VIJAY K.; GUVEN, OLGUN; MOURA, ESPERIDIANA A.B.Ethylene-vinyl alcohol (EVOH) copolymers are widely used in the food packaging industry as gas barrier properties to oxygen, organic solvents, and food aromas. EVOH is very sensitive to moisture and its gas barrier ability deteriorates in high relative humidity conditions. This work aims to prepare flexible films based on melt-blending high density polyethylene (HDPE) and ethylene-vinyl alcohol (HDPE/EVOH/EVA blend) reinforced with graphene oxide (GO). The HDPE/EVOH/EVA/GO flexible films were prepared by twin-screw extrusion and blown film extrusion processing. The flexible films samples were characterized by tensile tests, TG, DSC and FE-SEM analysis and the correlation between properties was discussed. In addition, the oxygen permeability tests were performed at 23 °C, 0 and 90% relative humidity using an OX-TRAN (MOCON Inc.).Artigo IPEN-doc 23863 Preparation and characterization of PBT/clay nanocomposite2012 - SARTORI, MARIANA N.; OLIVEIRA, RENE R.; DIAZ, FRANCISCO R.V.; ORTIZ, ANGEL V.; RANGARI, VIJAYA K.; MOURA, ESPERIDIANA A.B.This work presents the preparation and characterization of a nanocomposite based on Poly(butylene terephthalate) PBT and Brazilian smectitic clay (bentonite chocolate clay). Before being incorporated as clay nanoparticles in PBT resin, the clay was organically modified by the addition of a quaternary salt and sodium carbonate. PBT/Clay nanocomposite (96.3:3.70 wt %) was obtained by using a twin-screw extruder machine. After extrusion process, the nanocomposite was characterized by tensile, flexural and impact tests, SEM, Vicat, HDT, DSC, TGA and XRD tests. The results showed that the properties of the nanocomposite obtained were superior to those of neat PBT. Concerning the temperature of thermal distortion (HDT) an expressive gain of around 45 % was presented to PBT/Clay nanocomposite compared to PBT evidencing the interaction of nanofiller with the polymeric matrix.Artigo IPEN-doc 23881 Comparison between HDPE/clay and HDPE/piassava fiber/clay treated by electron beam radiation2013 - ORTIZ, ANGEL; ESCANHOELA, CORDELIA M.F.; GOMES, MICHELLE; OLIVEIRA, RENE R.; DIAZ, FRANCISCO R.V.; MOURA, ESPERIDIANA A.B.This work evaluates changes in morphological, mechanical and thermo-mechanical properties of electron-beam irradiated HDPE/nanoclay and HDPE/Piassava fiber/nanoclay. Material samples irradiated with 100 and 200 kGy using a 1.5 MeV electron beam accelerator (room temperature, presence of air) were submitted to tensile, flexural, and HDT tests. MFI, SEM and XRD analyses were carried out. Correlation between properties was discussed. Results showed that incorporation of piassava (Attalea funifera Mart) fiber and nanoclay, followed by irradiation represented significant gain in thermo-mechanical properties. Changes in surface morphology and reduction in MFI were observed. In conclusion, it may be claimed that the incorporation of piassava fiber in small size particles and nanoclay in the HDPE followed by electron-beam irradiation effectively improved the polymer properties and led to materials with superior properties suitable for several industrial applications.Artigo IPEN-doc 19383 Biodegradable aliphatic aromatic copolyester/corn starch blend composite reinforced with cofee parchment hush2013 - SILVA, VALQUIRIA A.; TEIXEIRA, JACIELE G.; GOMES, MICHELLE G.; ORTIZ, ANGEL V.; OLIVEIRA, RENE R.; SCAPIN, MARCOS A.; COLOMBO, MARIA A.; MOURA, ESPERIDIANA A.B.Artigo IPEN-doc 19381 Sugarcane bagasse ash reinforced HDPE composites: effects of electron-beam radiation crosslinking on tensile and porphological properties2013 - TEIXEIRA, JACIELE G.; GOMES, MICHELLE G.; OLIVEIRA, RENE R.; SILVA, VALQUIRIA A.; SARTORI, MARIANA M.; ORTIZ, ANGEL V.; MOURA, ESPERIDIANA A.B.Artigo IPEN-doc 20107 Preparation and characterization of electron-beam treated HDPE composites reinforced with rice husk ash and Brazilian clay2014 - ORTIZ, A.V.; TEIXEIRA, J.G.; GOMES, M.G.; OLIVEIRA, R.R.; DIAZ, F.R.V.; MOURA, E.A.B.