LETICIA MENDES DE OLIVEIRA

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  • Dissertação IPEN-doc 28497
    Datação de conchas e sedimentos do Sambaqui Gigante Santa Marta II, Laguna, Santa Catarina
    2019 - OLIVEIRA, LETICIA M. de
    Esse trabalho tem como objetivo determinar a idade de conchas e sedimentos de diferentes camadas do Sambaqui Santa Marta II, localizado na região de Laguna, Santa Catarina, Brasil. Foram coletadas amostras de conchas e sedimentos de camadas com diferentes profundidades, até o ponto mais próximo ao centro do sambaqui. Os sedimentos foram datados pelo método da Termoluminescência (TL). As conchas foram datadas pelo método de Ressonância Paramagnética Eletrônica (EPR), no laboratório de EPR - Universidade de Palermo, Itália, e duas amostras de conchas foram datadas por Radiocarbono, através da técnica de espectrometria de massa do acelerador (AMS) no laboratório Beta Analytic. Para reconstrução da dose acumulada, nas técnicas de TL e EPR, foi utilizado o método aditivo. A dose anual dos sedimentos de cada camada foi obtida através da técnica de espectroscopia gama, os resultados apresentaram valores entre 1,17 e 2,11 mGy/ano. As idades das conchas através do método EPR e Radiocarbono, considerando as incertezas, são aproximadamente de mesma ordem de grandeza, em torno de 3,3 mil anos. Apesar da profundidade estratigráfica dos sedimentos não ser diretamente proporcional às idades obtidas, provavelmente por conta do alto índice de destruição do Sambaqui, as idades obtidas são entre 2,0 e 4,0 mil. Os resultados das idades das conchas e sedimentos coletados na camada mais próxima ao centro do sambaqui são 3,8 e 4,1 mil anos respectivamente. É estimado que essa seja a idade inicial de construção do Sambaqui Santa Marta II.
  • Artigo IPEN-doc 27872
    EPR dating of sediments in the region of Iguape - Cananéia, Brazil
    2021 - CORTEZ, B.; CHUBACI, J.F.D.; GOMES, M.B.; MENDES, L.; ROCCA, R.R.; ARIZACA, E.C.E.; WATANABE, S.
    Dating of sediments was performed by physics method in this work. Natural radioactivity is present in sediments, and this method is based on the measurement of energy of radiation stored in the solid. Gamma irradiation of sediments create deffects in quartz structure that stores energy by the absorption of radiation. In the present work, Icapara sediment dating was done by Electron Paramagnetic Resonance (EPR) spectroscopy method. The intensity of EPR signal corresponding to the number of lattice defects with an unpaired electron in sediment quartz could be measured to estimate the accumulated dose of natural radiation and to calculate the geologic age. Located in the region of Iguape at southeast coast of São Paulo State, Icapara is a large sand terrace that was formed due to sea level fluctation that occurred more than 130 thousand years ago. Samples were taken from a point about 9 - 10 meters above the current control of the sea. Ages of 38,000 ±12,000 and 46,000 ± 7,000 years were obtained in this study by EPR analysis that are correlated with the Quaternary Period.
  • Artigo IPEN-doc 27230
    EPR dating of shells from Malhada Marsh, Rio de Janeiro, Brazil
    2020 - GOMES, M.B.; OLIVEIRA, L.M.; CORTEZ, B.; D'OCA, M.C.; TRANCHINA, L.; TOMARCHIO, E.; PARLATO, A.; CHUBACI, J.F.D.; GENNARI, R.; ROCCA, R.R.; D'ERRICO, F.; SOUSA, S.; WATANABE, S.; MARRALE, M.
    The formation of the coastal plain of the Brazilian sea is mainly due to the fl uctuation of relative sea level in the past. Armação dos Buzios or simply Buzios is a municipality in the microregion of lakes, in the state of Rio de Janeiro. In this region there is a lowland area about two meters above current sea level. This lowland area is also known as coastal plain of Una River. It is expected that during the Holocene period the sea level reached a maximum about 2.5 meters above the current level. During that time billions of mollusks lived and proliferated in the shallow waters around the coastal plain of the Una River. As they died their shells formed a layer in the soil including Malhada Marsh that belongs to the Una River plain. In this study, shells were collected from this region and dated using the techniques of Electronic Paramagnetic Resonance (EPR). Ages from 2480±130 to 4490±270 years were obtained. Radiocarbon dating were performed at the Beta Analytic Lab, USA for comparison with the EPR results. Shells ages obtained are compatible with geological data from the Holocene period relative to past sea level fl uctuations.
  • Artigo IPEN-doc 27229
    Electron Spin Resonance and Thermoluminescence dating of shells and sediments from Sambaqui (shell mound) Santa Marta II, Brazil
    2020 - OLIVEIRA, L.M.; GOMES, M.B.; CORTEZ, B.; D'OCA, M.C.; TRANCHINA, L.; TOMARCHIO, E.; PARLATO, A.; CHUBACI, J.F.D.; GENNARI, R.; ROCCA, R.R.; D'ERRICO, F.; SOUSA, S.; WATANABE, S.; MARRALE, M.
    In Tupi, the word Sambaqui means “mound of shells”. These archaeological sites are cultural vestiges left by the prehistoric occupation of the Brazilian coast from fi ve to six thousand years ago. Mollusks, fi shes, and other marine edible foods were important for the survival of this population. The remains of foods, mainly shells, were heaped up, giving a mound of different proportions, which became part of the landscape of the Brazilian coastal plain. Due to the large number of Sambaquis in Brazil and considering that Sambaqui Santa Marta II, Laguna, SC, has not yet been dated, Electron Spin Resonance (ESR) measurements were performed in aragonite shells collected from different layers of Sambaqui Santa Marta II, starting from the base to the center of the Sambaqui. Radiocarbon analysis by Accelerator Mass Spectrometry (AMS) at Beta Analytic laboratory were also performed for comparison with ESR results. Before measurements, shells were chemically etched, after drying, were pulverized and sieved. The sediments were separated into small portions which were irradiated with gamma radiation from a 60Co source with doses from 5 up to 120 Gy. Ages around 2,000 to 4,000 years have been obtained. The results obtained are consistent with the dates of others Sambaquis of the region, possibly were built at the same time.
  • Resumo IPEN-doc 26028
    Dating sediments from a terrace found in Iguape - Icapara in southeast coast in the state of São Paulo, Brazil
    2018 - CORTEZ, BRUNA; CHUBACI, JOSE F.D.; GOMES, MONISE B.; OLIVEIRA, LETICIA M.; SATIRO, LUCAS C.; ROCCA, RENE R.; ARIZACA, EDY E.C.; WATANABE, SHIGUEO
  • Resumo IPEN-doc 26027
    Dating of shells from Pântano da Malhada, Rio de Janeiro
    2018 - GOMES, MONISE B.; CORTEZ, BRUNA; OLIVEIRA, LETICIA M. de; CARMO, LUCAS S. do; CHUBACI, JOSE F.D.; ROCCA, RENE R.; WATANABE, SHIGUEO
  • Artigo IPEN-doc 25836
    TL in green tourmaline
    2019 - CANO, NILO F.; RAO, T.K.G.; AYALA-ARENAS, JORGE S.; GONZALES-LORENZO, CARLOS D.; OLIVEIRA, LETICIA M.; WATANABE, SHIGUEO
    Electron paramagnetic resonance (EPR) studies have been carried out to identify the defect centers responsible for the thermoluminescence (TL) peaks in the mineral tourmaline. The mineral exhibits three TL peaks approximately at 170, 250 and 310 °C. The EPR spectrum of the green tourmaline sample pre-heated to 500 °C presented a large signal around g=4.3 due to Fe3+ ion. Room temperature EPR spectrum of irradiated green tourmaline shows the formation of two defect centers in the region of g=2.0. One of the centers (center II) with a g factor equal to 1.96 is identified as an F+-center and is related to the observed high temperature 250 and 310 °C TL peaks. Center I exhibiting a doublet is due to hydrogen atoms (H0), stable in the crystal lattice at room temperature and this center correlates with the TL peak at 170 °C of the green tourmaline. An optical absorption measurement also was carried out. Bands at around 430, 730 and 1100 nm have been observed.
  • Artigo IPEN-doc 22588
    Gamma irradiation effects on poly(hydroxybutyrate)
    2006 - OLIVEIRA, LETICIA M.; ARAUJO, ELMO S.; GUEDES, SELMA M.L.