LAISSA ADRIANA BONIFACIO DOS SANTOS

LAISSA ADRIANA BONIFACIO DOS SANTOS

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Inorganic chemical composition by X-ray fluorescence spectrometry of the mineral waters from the Minas Gerais Water Circuit, Brazil
2021 - WAKASUGI, D.S.M.; DAMATTO, S.R.; MENEGHINI, A.A.; SANTOS, L.A.B.; SALVADOR, V.L.R.
The water parks located in the cities of Cambuquira, Caxambu, Conceição do Rio Verde, Lambari and Marimbeiro are part of the Water Circuit of Minas Gerais and have their mineral waters regularly consumed by the local population and tourists motivated by the medicinal use of these waters, characterized as mineral waters. Therefore, the objective of this work was to determine the inorganic chemical composition of the mineral water from these parks, analysing the elements Ag, As, Ba, Ca, Cd, Co, Cr, Cu, Fe, K. Mn, Ni, Pb, Se, Ti, V and Zn using the energy dispersive X-ray fluorescence – EDXRF. Despite the proximity to one another, each park has different chemical elements and concentrations. The elements presenting the highest concentrations were the major elements Ca, Fe, K and Mn. However, among the five water parks studied, the Water Park of Caxambu presented the highest concentrations for all the determined elements.
Inorganic chemical elements determined in mineral water springs from the water circuit of Minas Gerais, Brazil by X-ray fluorescence spectrometry
2019 - MENEGHINI, ARTHUR A.; WAKASUGI, DENISE S.M.; SANTOS, LAISSA A.B. dos; DAMATTO, SANDRA R.; SALVADOR, VERA L.R.
Water Circuit of Minas Gerais (Circuito das Águas de Minas Gerais) is known by its mineral water parks located in the cities of Cambuquira, Caxambu, Conceição do Rio Verde, Lambari and São Lourenço. The mineral water of these parks is consumed regularly by the local population and tourists that are motivated by the medicinal use of the mineral water. One of the characteristics that defines a mineral water is its chemical composition, hence a water is considered mineral due to the chemical elements present in its composition. The objective of this work was to determine the inorganic chemical characterization of the mineral waters from the Water Parks of Cambuquira, Caxambu, Conceição do Rio Verde, Lambari and Marimbeiro analyzing the elements Ag, As, Ba, Ca, Cd, Co, Cr, Cu, Fe, K. Mn, Ni, Pb, Se, Ti, V and Zn by energy dispersive X-ray fluorescence spectrometry – EDXRF. Each water park presented different chemical elements with different concentrations, in spite of the parks are located near each other. The elements that presented the highest concentrations in all the samples analyzed were the major elements Ca, Fe, K and Mn. Among the four water parks studied, the mineral waters from Water Park of Caxambu presented the highest concentrations for all the elements determined. This study is part of a research project developed at CMR that studied the natural radionuclides 226Ra, 228Ra, 210Pb and 210Po and the inorganic chemical elements of the mineral waters of the Water Circuit of Minas Gerais.
Avaliação das concentrações dos radionuclídeos 226Ra, 228Ra, 210Pb, 210Po e caracterização química inorgânica das águas minerais do Parque das Águas de Cambuquira e Marimbeiro, MG
2018 - SANTOS, LAÍSSA A.B. dos
A exposição a fontes naturais de radiação contribui com mais de 98% da dose de radiação normalmente recebida da população; esta dose é principalmente atribuída à incorporação de radionuclídeos naturais das séries de decaimento do 238U e 232Th que possuem meia-vidas relativamente longas. A qualidade da água para consumo humano deve ser constantemente analisada e, um parâmetro muito importante analisado é a radioatividade natural presente. Quando os radionuclídeos naturais estão presentes em águas minerais há uma maior preocupação, pois estas águas podem conter concentrações moderadamente elevadas de 226Ra, 228Ra e 222Rn originalmente dissolvidas e dos radionuclídeos 210Pb e 210Po, que embora apresentem menores concentrações, contribuem para um aumento da irradiação interna e externa dos indivíduos. As áreas de estudo do presente trabalho foram os Parques das Águas de Cambuquira e Marimbeiro e de uma fonte particular de uma fazenda localizados na cidade de Cambuquira, Minas Gerais, onde as águas minerais são frequentemente utilizadas para consumo humano e uso médico. Assim, o objetivo deste trabalho foi determinar as concentrações de atividade dos radionuclídeos 226Ra, 228Ra e 210Pb e 210Po, avaliar as doses efetivas comprometidas devido ao consumo e fazer a caracterização química inorgânica destas águas minerais. Os radionuclídeos foram determinados por medida alfa e beta total e espectrometria alfa, após separação radioquímica em coletas realizadas sazonalmente. Para a caracterização química inorgânica foram determinadas as concentrações dos elementos As, Ag, Ba, Ca, Cd, Co, Cr, Cu Fe, K, Mn, Ni, Se, Ti e V por fluorescência de raios X. As concentrações de atividades dos radionuclídeos variaram de 4 ± 1 mBq/l a 509 ± 32 mBq/l para 226Ra, de 3,7 ± 0,1 mBq/l a 631 ± 27 mBq/l para 228Ra, de 5 ± 1 mBq/l a 60 ± 5 mBq/l para 210Pb e de abaixo do limite de detecção da metodologia a 36 ± 2 mBq/l para o 210Po. A dose efetiva comprometida máxima em adultos foi de 0,12 mSv/a para 226Ra, 0,32 mSv/a para 228Ra, 0,03 mSv/a para 210Pb e para 210Po 0,031 mSv/a. Dentre os elementos analisados por fluorescência de raios X, os elementos Ag, As, Cd, Cr, Cu, Ni, Se e Ti apresentaram valores abaixo do limite mínimo de detecção da metodologia. Os elementos Ba e Co, considerados contaminantes nas águas minerais, apresentaram valores maiores do que estabelecido pela ANVISA e CONAMA para águas minerais, respectivamente. No entanto, trabalhos da literatura brasileira realizados com água mineral de em outros locais apresentaram valores próximos ao do presente estudo, mostrando que concentrações acima do limite podem representar uma anomalia natural do aquífero.
Variação sazonal das concentrações de 226Ra, 228Ra e 210Pb das fontes de água mineral do Parque das Águas de Cambuquira e Marimbeiro, MG
2017 - SANTOS, LAISSA A.B. dos; DAMATTO, SANDRA R.; OLIVEIRA, JOSELENE de
Os elementos radioativos podem sem extraídos e arrastados pelas águas subterrâneas, porém quando se fala de águas minerais provindas de fontes subterrâneas uma característica marcante são as concentrações dos radionuclideos 226Ra e 222Rn originalmente dissolvidos. No entanto, outros radionuclídeos naturais como 228Ra e 210Pb, quando presentes, também contribuem para a irradiação interna do individuo. Assim determinou-se as concentrações de 226Ra, 228Ra e 210Pb em dez fontes minerais localizadas no Parque das Águas de Cambuquira e Marimbeiro. Os radionuclideos foram determinados por procedimento radioquimico em quatro coletas em diferentes estações do ano. As concentrações variaram de 4 ±1 mBq/L a 509 ± 32 mBq/L para 226Ra, de < 3,7 ± 0,1 mBq/L a 594 ±35 mBq/L para 228Ra e 5 ± 1 mBq/L a 59 ± 4 mBq/L para 210Pb.
Use of INAA technique in mineral water samples from the Parque das Águas of Cambuquira and Marimbeiro
2017 - SANTOS, L.A.B.; SHIGASI, A.; DAMATTO, S.R.
Water is an indispensable molecule for the existence of life, thus several studies analyze both their chemical composition and biological and radiological. There is a greater concern about mineral waters, since they tend to be consumed even as a therapeutic form, originating the study of crenotherapy. Currently there are several analytical techniques for the determination of elements in water and one that can be used is the neutron activation analysis, which consists of a technique that forms radioactive isotopes by means of reactions that occur in the nucleus of the atoms, thus allowing simultaneous determination of various chemical element concentrations. In addition to being a sensitive and reliable method, it is free of sample destruction. The method can be used either in samples in their solid or liquid form. The mineral water, according to Decree Law No. 7.841 of 08.08.1945 is defined as: "Mineral waters are those from natural or artificially collected sources that have chemical composition or physical or physico-chemical properties distinct from common waters with characteristics that give them a medication action". In addition to chemical composition, these waters may be classified by other physical chemical characteristics, such as temperature and gases; they are also studied in the field of medicine. The objective of this study was to determine the concentration of the elements As, Ba, Br, Ca, Ce, Co, Cr, Cs, Eu, Fe, Hf, K, La, Lu, Na, Nd, Rb, Sb, Sc, Se, Sm, Ta, Tb, Th, U, Yb and Zn in the mineral waters from Parque das Águas of Cambuquira, springs Gasosa I, II and III, Férrea, Magnesiana, Litinada and Marimbeiro springs 1, 2 and 3, both parks located in the city of Cambuquira, MG. Parque das Águas of Marimbeiro is located 3km from the center of the city of Cambuquira; the parks are managed by the CODEMIG. A sample of a mineral water spring was also collected from a private property open to the population, near to the park of Cambuquira and called the spring of Laranjal or Dico. The samples for the autumn sampling of 2016 were analyzed, for which the results obtained showed that in the mineral waters of the parks Cambuquira and Marimbeiro was determined the elements Na and Ca, which are expected elements since an important characteristic of fresh waters is that they have an identity of the inorganic ions. This characteristic may be linked to the salts of these ions being moderately soluble, thus facilitating their mobilization in aqueous medium. Also determined in the waters were the elements Zn, Co, Fe and rare earth elements such as Sm and La.
Determination of the 226Ra, 228Ra AND 210Pb concentrations in the mineral water springs from water parks of Cambuquira and Marimbeiro, Minas Gerais and assessment of the committed effective doses
2017 - SANTOS, LAISSA A.B. dos; DAMATTO, SANDRA R.
Due to the importance of human life, water quality must be controlled and a very important parameter are the limits of the natural radioactivity of the water consumed.In relation to therapeutic practices based on water intake the radionuclides 210Pb , 226Ra and 228Ra when present, are of great importance because they contribute to the internal irradiation of individuals.The study areas of the present work were the Parque das águas of Cambuquira and Marimbeiro, located in Minas Gerais. Hence, the objective of this work was to determine the 226Ra, 228Ra and 210Pb concentrations in the springs of these parks and evaluate the committed effective doses due to its consumption.The radionuclides were determined by a radiochemical procedure in four collections at different seasons of the year. The Concentrations ranged from 4 ± 1 mBq / L to 509 ± 32 mBq / L for 226Ra, from 3.7 ± 0.1 mBq / L to 631 ± 27 mBq / L for 228Ra and 5 ± 1 mBq / L to 60 ± 5 mBq / L for 210Pb. The dose for adults from 1.21x10-01 mSv/y for 226Ra, 3.18x10-01 mSv/y for 228Ra and for 210Pb 3.02x10-02 mSv/y.
Preliminary results of 226Ra, 228Ra and 210Pb concentration in mineral waters from Parque das Águas de Cambuquira and Marimbeiro (MG)
2016 - SANTOS, LAISSA A.B. dos; DAMATTO, SANDRA R.; OLIVEIRA, JOSELENE de; CARMO, AMANDA P. do