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  • Artigo IPEN-doc 27977
    Development of methodologies for decontamination, reuse and improvement of the properties of respiratory protective equipment using ionizing radiation
    2020 - VASQUEZ, P.A.S.; MORAIS, F.; LIMA, F.S.; SANTOS, P.S.; MORAES, O.; ARTAXO, P.; JOHN, V.M.; NAGAI, M.L.E.; OLIVEIRA, M.J.A.; CATALANI, L.H.; KODAMA, Y.; OTUBO, L.
  • Artigo IPEN-doc 26299
    Effect of ionizing radiation on the color of featherwork
    2019 - VIEIRA, ANA C.D.; KODAMA, YASKO; OTUBO, LARISSA; SANTOS, PAULO de S.; VASQUEZ, PABLO A.
    Featherwork collections are usually stored and managed by ethnographic museums. Even though the featherwork manufacturing is still practiced by the indigenous communities, the offer of raw material and the contact with the surrounding society ended up reducing the production scale of such objects. Consequently, the preservation of the culture heritage is very important, particularly in museums. Biodegradation can affect featherworks mainly by xylophagous insects and moths’ action. The tropical Brazilian weather contributes to the contamination and proliferation of insects and fungi making the preservation conditions difficult. The use of gamma radiation for the disinfection of cultural heritage objects and archived materials has shown to be a safe process and an excellent alternative to traditional methods usually involving high persistent and toxic chemical pesticides. In this work are presented the preliminary results of the ionizing radiation effects on the color and morphological properties of a featherwork from the Museum of Archeology and Ethnology of the University of São Paulo (MAE/USP). Samples of feathers were selected from the artifact and irradiated with gamma rays at the Multipurpose Gamma Irradiation Facility at IPEN, applying absorbed doses between 0.5 kGy to 200 kGy. Samples were firstly chosen according to feather colors, photographed and analyzed using colorimetry with CIELAB 1976 color space scale and scanning electron microscopy (SEM), just after and 48 hours after the irradiation process. The results shown had no significant changes on color and morphological properties within the disinfection absorbed dose range applied.
  • Artigo IPEN-doc 26298
    Effect of ionizing radiation on the color of botanical collections
    2019 - LIMA, LENI M.P.R.; KODAMA, YASKO; OTUBO, LARISSA; SANTOS, PAULO de S.; VASQUEZ, PABLO A.
    Conservation and preservation strategies are essential to manage botanical collections specially for dried herbarium specimens also known as exsiccates, usually referring to a set of identified specimens belonging to taxa and distributed among all herbaria around the world. Particularly, these collections are very sensitive to the attack of fungi and insects. In recent years, disinfection by ionizing radiation has become an effective strategy to preserve cultural heritage objects and archived materials with excellent results. In this work, the effects on color properties of gamma radiation on exsiccates samples were studied. Thus, six exsiccates, botanical pressed and dehydrated samples were selected from the Dom Bento José Pickel Herbarium (SPSF), situated at São Paulo (Brazil). Three of these samples comes from Asteraceae family and were collected in 1946, 1984 and 1986, while three other samples belong to Solanaceae family and were collected in 1953, 1984 and 2007. Families of selected botanical collections are very susceptible to biodegradation. The irradiation was performed at the Multipurpose Gamma Irradiation Facility at IPEN applying absorbed doses of 1 kGy, 6 kGy and 10 kGy, which are values of absorbed dose for disinfestation and disinfection. Results were analyzed using colorimetry with CIELAB color space scale and scanning electron microscopy. The results showed that there were no significant changes on colorimetric morphological properties of the samples.
  • Artigo IPEN-doc 24036
    Preservation of photographic and cinematographic films by gamma radiation- preliminary analyses
    2017 - NAGAI, MARIA L.E.; SANTOS, PAULO S.; OTUBO, LARISSA; OLIVEIRA, MARIA J.A.; VASQUEZ, PABLO A.S.
    Brazilian weather conditions affect directly tangible materials causing deterioration notably getting worse by insects and fungi attack. In this sense, gamma radiation provided from the cobalt-60 is an excellent alternative tool to the traditional preservation process mainly because it has biocidal action. Radiation processing using gamma radiation for cultural heritage materials for disinfection has been widely used around the world in the last decades. Many cultural heritage objects especially made on paper and wood were studied in scientific publications aiming mechanical, physical and chemical properties changes. Over the last fifteen years, the Multipurpose Gamma Irradiation Facility of the Nuclear and Energy Research Institute located inside the Sao Paulo University campus has been irradiated many collections of archived materials, books, paintings and furniture. Adequate storage of photographic and cinematographic materials is a challenge for conservators from preservation institutions. Contamination by fungi is one of leading causes of problem in photographic and cinematographic collections. Several Sao Paulo University libraries have been affected by fungi in their photographic and cinematographic collections making it impossible to research on these materials either manipulate them for health and safety reasons. In this work are presented preliminary results of effects of the ionizing radiation in photographic and cinematographic films. Selected film samples made on cellulose acetate were prepared and characterized by FTIR-ATR spectroscopy. Samples were irradiated by gamma rays with absorbed dose between 2 kGy and 50 kGy. Irradiated samples were analyzed by UV-VIS spectroscopy and electron microscopy techniques. Results shown that disinfection by gamma radiation can be achieved safely applying the disinfection dose between 6 kGy to 15 kGy with no significant change or modification of main properties of the constitutive materials.