FAUZE JACÓ ANAISSI

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2011 - 20132
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    Artigo IPEN-doc 17632
    Produção de hibridos Ni/carbono por carbonização hidrotérmica para aplicação como suportes de eletrocatalisadores PtRu/C usados na oxidação eletroquímica do metanol
    2011 - TUSI, MARCELO M.; POLANCO, NATALY S.O.; BRANDALISE, MICHELE; SILVA, ANTONIO C.; CORREA, OLANDIR V.; VILLALBA, JUAN C.; ANAISSI, FAUZE J.; OLIVEIRA NETO, ALMIR; SPINACE, ESTEVAM V.
  • Imagem de Miniatura
    Artigo IPEN-doc 19057
    Ni/Carbon hybride prepared by hydrothermal carbonization and thermal treatment as support for PtRu nanoparticles for direct methanol fuel cell
    2013 - TUSI, MARCELO M.; BRANDALISE, MICHELE; POLANCO, NATALY S. de O.; CORREA, OLANDIR V.; SILVA, ANTONIO C. da; VILLALBA, JUAN C.; ANAISSI, FAUZE J.; OLIVEIRA NETO, ALMIR; SPINACE, ESTEVAM V.
    Ni/Carbon was prepared in two steps: initially cellulose as carbon source and NiCl2$6H2O as catalyst of the carbonization process were submitted to hydrothermal treatment at 200 C and further to thermal treatment at 900 C under argon atmosphere. The obtained material contains Ni nanoparticles with face-centered cubic (fcc) structure dispersed on amorphous carbon with graphitic domains. PtRu/C electrocatalysts (carbonsupported PtRu nanoparticles) were prepared by an alcohol-reduction process using Ni/Carbon as support. The materials were characterized by thermogravimetric analysis, energy-dispersive X-ray spectroscopy, Fourier transform infrared spectroscopy, X-ray diffraction, transmission electron microscopy and tested as anodes in single direct methanol fuel cell (DMFC). The performances of PtRu/C electrocatalysts using Ni/Carbon as support were superior to those obtained for PtRu/C using commercial carbon black Vulcan XC72 as support.