DANIEL RICCO ELIAS
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Resumo IPEN-doc 19088 Synthesis of lanthanum silicate oxyapatite ceramic powder as a solid oxide fuel cell electrolyte by a new modified sol gel method2013 - ELIAS, DANIEL R.; LIRA, SABRINA L.; PAIVA, MAYARA R.S.; MISSO, AGATHA M.; YAMAGATA, CHIEKOArtigo IPEN-doc 18441 Síntese de pós de Lasub(9,56)(SiOsub(4))sub(6)Osub(2,34) e Lasub(9,8)Sisub(5.7)Mgsub(0.3)Osub(26,4) por processo sol-gel modificado2012 - LIRA, SABRINA L.; PAIVA, MAYARA R.S.; MISSO, AGATHA M.; ELIAS, DANIEL R.; YAMAGATA, CHIEKOArtigo IPEN-doc 18918 Influence of the precursor concentration on the characteristics of silica powder obtained from Nasub(2)SiOsub(3) by a facile low temperature synthesis process2012 - YAMAGATA, CHIEKO; ELIAS, DANIEL R.; PAIVA, MAYARA R.S.; MISSO, AGATHA M.; MELLO CASTANHO, SONIA R.H.Artigo IPEN-doc 19079 Facile preparation of apatite-type lanthanum silicate by a new water-based sol-gel process2013 - YAMAGATA, CHIEKO; ELIAS, DANIEL R.; PAIVA, MAYARA R.S.; MISSO, AGATHA M.; CASTANHO, SONIA R.H.M.In recent years, apatite-type lanthanum silicates ([Ln10x(XO4)6O3–1.5x] (X = Si or Ge)) have been studied for use in SOFC (solid oxide fuel cells), at low temperature (600–800 8C), due to its ionic conductivity which is higher than that of YSZ (Yttrium Stabilized Zirconia) electrolyte. For this reason they are very promising materials as solid electrolyte for SOFCs. Synthesis of functional nanoparticles is a challenge in the nanotechnology. In this work, apatite-type lanthanum silicate nanoparticles were synthesized by a water-based sol–gel process, i.e., sol–gel technique followed by chemical precipitation of lanthanum hydroxide on the gel of the silica. Na2SiO3 waste solution was used as silica source. Spherical aerogel silica was prepared by acid catalyzed reaction, followed by precipitation of lanthanum hydroxide to obtain the precursor of apatite-type lanthanum silicate. Powders of apatite-type lanthanum silicate achieved from the precursor were characterized by thermal analysis, X-ray diffraction (XRD), scanning electron microscopy (SEM) and specific surface area measurements (BET). The apatite phase was formed at 900 8C.