SOLANGE KAZUMI SAKATA

SOLANGE KAZUMI SAKATA

(Fonte: Lattes)

Resumo

Possui graduação em Química bacharelado e licenciatura pela Universidade de São Paulo. Doutorado na área de Química Orgânica, com ênfase em Eletrossintese Orgânica pelo Instituto de Química da Universidade de São Paulo. Pós - doutorados em Biotecnologia no Scripps Institution of Oceanography na University of California - San Diego -USA) e no Instituto de Química da Universidade de São Paulo. Foi pesquisadora visitante no Fraunhofer Institute for Interfacial Engineering and Biotechnology IGB-Stuttgart - Alemanha no estudo do metagenoma na produção de enzimas para fins catalíticos e no Centro Tecnológico da Marinha de São Paulo (CTM-SP) no desenvolvimento e caracterização de polímeros. Atualmente é pesquisadora do Instituto de Pesquisas Energéticas e Nucleares (IPEN- SP / CNEN) no Centro de Tecnologia das Radiações e estuda o efeitos das radiações em nano materiais de carbono. (Texto extraído do Currículo Lattes em 27 dez. 2021).

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Low-temperature reduction of graphene oxide using the HDDR process for electrochemical supercapacitor applications
2020 - BENITEZ JARA, F.G.; CRUZ, P.D.V.; BARBOSA, L.P.; CASINI, J.C.S.; SAKATA, S.K.; PERUZZI, A.J.; FARIA, R.N.
In the present work, attempts of reducing a graphene oxide powder using a low temperature hydrogenation disproportionation desorption and the recombination process (L-HDDR) has been carried out. A lower processing temperature in large scale production is significant when costs are concerned. Graphite oxide was prepared using a modified Hummers’ method dispersed in ethanol and exfoliated using ultrasonication to produce Graphene Oxide (GO). Investigations have been carried out by X-ray diffraction (XRD) and scanning electron microscopy (SEM). The experimental results of L-HDDR processing graphene oxide powder, using unmixed hydrogen at 400°C and relatively low pressures (<2 bars) have been reported. X-ray diffraction patterns showed a reduction of graphene oxide with the L-HDDR process. The results showed that both processes, the L-HDDR as well as the standard HDDR, may be applied to the reduction of graphene oxide in order to produce supercapacitor materials. The advantage of employing the L-HDDR process is a relatively low temperature reducing the cost of treatment, what is a very important factor for producing a large amount of material. Thus, the L-HDDR process has been considered a promising alternative method of reducing graphene oxide with efficiency, with the possibility of large scale production.
Supercapacitor application of powder prepared using the Hydrogenation Disproportionation Desorption and Recombination (HDDR) process in graphene oxide
2017 - CASINI, JULIO C.S.; FERNANDEZ, ANTONIO P.R.; OLIVEIRA, RENE R. de; SAKATA, SOLANGE K.; FARIA JUNIOR, RUBENS N.
Graphene (G) has been attracted great interest for its excellent electrical properties. However, the large-scale production of graphene is presently unfeasible. Graphene oxide (GO) can be (partly) reduced to graphene-like sheets by removing the oxygen-containing groups with the recovery of a conjugated structure. It can be produced using inexpensive graphite as raw material by cost-effective chemical methods. Although hydrogen (mixed with argon) at high temperature (1100°C) has been employed to reduce GO powder, the hydrogenation disproportionation desorption and recombination (HDDR) process in particular was unreported for this purpose. In the present work, attempts of reducing GO powder using the HDDR process have been carried out and investigated by X-ray diffraction (XRD), scanning electron microscopy (SEM) thermogravimetric analysis (TGA) and Fourier transform infrared spectroscopy (FTIR). The experimental results of processing graphene oxide powder using unmixed hydrogen at moderate temperatures (about 850°C) and relatively low pressures (<2 bars) have been reported.