CECILIA CHAVES GUEDES E SILVA

Resumo

Possui graduação em Engenharia de Materiais pela Universidade Presbiteriana Mackenzie (1997), mestrado em Tecnologia Nuclear Aplicações pelo Instituto de Pesquisas Energéticas e Nucleares (2000) e doutorado em Tecnologia Nuclear Materiais pelo Instituto de Pesquisas Energéticas e Nucleares (2005). Atualmente é pesquisador do Instituto de Pesquisas Energéticas e Nucleares. Tem experiência na área de Engenharia de Materiais, atuando principalmente nos seguintes temas: materiais cerâmicos, biomateriais e materiais nucleares. (Texto extraído do Currículo Lattes em 08 out. 2021)

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  • Artigo IPEN-doc 30825
    Exfoliation of titanium nitride using a non-thermal plasma process
    2024 - ZAMBIAZI, PRISCILA J.; LAZAR, DOLORES R.R.; OTUBO, LARISSA; SOUZA, RODRIGO F.B. de; OLIVEIRA NETO, ALMIR; GUEDES-SLVA, CECILIA C.
    In this study, we present a novel approach for the exfoliation of titanium nitride (TiN) powders utilizing a rapid, facile, and environmentally friendly non-thermal plasma method. This method involves the use of an electric arc and nitrogen as the ambient gas at room temperature to generate ionized particles. These ionized species interact with the ceramic crystal of TiN, resulting in a pronounced structural expansion. The exfoliated TiN products were comprehensively characterized using transmission electron microscopy, X-ray diffraction, and Raman spectroscopy. Remarkably, the cubic crystal structure of TiN was effectively retained, while the (200) crystal plane d-spacing increased from 2.08 to 3.09 Å, accompanied by a reduction in crystallite size and alterations in Raman vibrational modes. Collectively, these findings provide compelling evidence for the successful exfoliation of TiN structures using our innovative non-thermal plasma method, opening up exciting possibilities for advanced material applications.