X-ray diffraction and thermoanalytical datasets of precursors of the Gd6UO12-δ phase processed by combined mechanochemical
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2021
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Data in Brief
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The datasets presented here are related to the research paper entitled “Disordered Gd6UO12-δ with the cation antisite defects prepared by a combined mechanochemical−thermal method” [1]. The datasets complement the findings [1] on the effect of the combined mechanochemical−thermal processing of the stoichiometric mixture of solid precursors (3Gd2O3 + UO2) on the formation of Gd6UO12-δ phase. In this article, we provide (i) X-ray diffraction (XRD) data of the 3Gd2O3 + UO2 mixture milled for 12 h, (ii) the refined XRD data of the non-milled 3Gd2O3 + UO2 mixture after annealing at 1282 °C for 3 h in air, and (iii) the thermogravimetric and differential thermal analysis (TG-DTA) data for non-milled and mechanically preactivated 3Gd2O3 + UO2 mixture measured in air at a heat rate of 10 K/min.
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DARIN, GASPAR; IMAKUMA, KENGO; SANTIAGO, RAFAEL T.; SILVA, KLEBSON L. da; COTICA, LUIZ F.; FABIAN, MARTIN; VALICEK, JAN; HAHN, HORST; SEPELAK, VLADIMIR. X-ray diffraction and thermoanalytical datasets of precursors of the Gd6UO12-δ phase processed by combined mechanochemical: thermal routes. Data in Brief, v. 35, p. 1-5, 2021. DOI: 10.1016/j.dib.2021.106972. Disponível em: http://repositorio.ipen.br/handle/123456789/32010. Acesso em: 12 Feb 2025.
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