Three routes for the synthesis of the bioceramic powder of the CaO-MgO-SiO2 system

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dc.contributor.authorYAMAGATA, CHIEKOpt_BR
dc.contributor.authorLEME, DANIEL R.pt_BR
dc.contributor.authorRODRIGUES, VANESSA G.pt_BR
dc.contributor.authorERETIDES, GABRIEL T.pt_BR
dc.contributor.authorRODAS, ANDREA C.D.pt_BR
dc.coverageInternacionalpt_BR
dc.date.accessioned2022-04-19T13:42:09Z
dc.date.available2022-04-19T13:42:09Z
dc.date.issued2022pt_BR
dc.description.abstractWe report three routes for the synthesis of CaO-MgO-SiO2 (CMS) bioceramic powder using different Si sources and synthesis procedures. The ceramic powders were synthesized from Na2SiO3 waste solution by the sol-gel process combined with co-precipitation (synthesis route I and synthesis route II), and from TEOS (tetraethyl orthosilicate) by conventional sol-gel (synthesis route III). Ceramic powders of the CMS multiphase system were obtained, including diopside, wollastonite, akermanite, monticellite and merwinite, which are suitable for application as biomaterial. These powders were sintered at 1200 °C for 2 h to obtain the CMS ceramics. The ceramics mostly contained diopside and wollastonite crystalline phases. Those ceramics when submitted to cytotoxicity tests revealed to be non-cytotoxic, according to ISO10993-5:2009. The ceramics were tested for in vitro bioactivity while soaked in simulated body fluid (SBF) solution. After 14 days, the presence of hydroxyapatite particles on the surface of ceramics was confirmed by Fourier Transform Infrared (FTIR) spectroscopy and Scanning Electron Microscopy (SEM) micrographs. The surfaces were completely covered with hydroxyapatite, after 21 days. In summary, CaO-MgO-SiO2 (CMS) ceramic powder derived from three routes of synthesis have potential application in the biomedical area. However, further in-vitro and in-vivo studies are needed.pt_BR
dc.description.sponsorshipFundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)pt_BR
dc.description.sponsorshipIDFAPESP: 18/10114-7pt_BR
dc.format.extent9681-9691pt_BR
dc.identifier.citationYAMAGATA, CHIEKO; LEME, DANIEL R.; RODRIGUES, VANESSA G.; ERETIDES, GABRIEL T.; RODAS, ANDREA C.D. Three routes for the synthesis of the bioceramic powder of the CaO-MgO-SiO2 system. <b>Ceramics International</b>, v. 48, n. 7, p. 9681-9691, 2022. DOI: <a href="https://dx.doi.org/10.1016/j.ceramint.2021.12.169">10.1016/j.ceramint.2021.12.169</a>. Disponível em: http://repositorio.ipen.br/handle/123456789/32962.
dc.identifier.doi10.1016/j.ceramint.2021.12.169pt_BR
dc.identifier.fasciculo7pt_BR
dc.identifier.issn0272-8842pt_BR
dc.identifier.orcid0000-0002-0967-0807pt_BR
dc.identifier.percentilfi91.1pt_BR
dc.identifier.percentilfiCiteScore83.8pt_BR
dc.identifier.urihttp://repositorio.ipen.br/handle/123456789/32962
dc.identifier.vol48pt_BR
dc.relation.ispartofCeramics Internationalpt_BR
dc.rightsopenAccesspt_BR
dc.subjectsynthesis
dc.subjectceramics
dc.subjectbiological materials
dc.subjectsol-gel process
dc.subjectcoprecipitation
dc.titleThree routes for the synthesis of the bioceramic powder of the CaO-MgO-SiO2 systempt_BR
dc.typeArtigo de periódicopt_BR
dspace.entity.typePublication
ipen.autorDANIEL DE REZENDE LEME
ipen.autorGABRIEL TRINDADE ERETIDES
ipen.autorVANESSA GALVAO RODRIGUES
ipen.autorCHIEKO YAMAGATA
ipen.codigoautor14114
ipen.codigoautor14471
ipen.codigoautor11690
ipen.codigoautor177
ipen.contributor.ipenauthorDANIEL DE REZENDE LEME
ipen.contributor.ipenauthorGABRIEL TRINDADE ERETIDES
ipen.contributor.ipenauthorVANESSA GALVAO RODRIGUES
ipen.contributor.ipenauthorCHIEKO YAMAGATA
ipen.date.recebimento22-04
ipen.identifier.fi5.2pt_BR
ipen.identifier.fiCiteScore8.8pt_BR
ipen.identifier.ipendoc28662pt_BR
ipen.identifier.iwosWoSpt_BR
ipen.range.fi4.500 - 5.999
ipen.range.percentilfi75.00 - 100.00
ipen.type.genreArtigo
relation.isAuthorOfPublication95a9457c-7834-4665-9c55-3f82573a458c
relation.isAuthorOfPublication20318f6b-50ca-4057-ae1b-f5c2eed5f57f
relation.isAuthorOfPublication82a932b6-4482-41a7-a6c8-c2741a3a157c
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relation.isAuthorOfPublication.latestForDiscovery9a4bd34a-7406-42f3-8741-5c934840fdc9
sigepi.autor.atividadeERETIDES, GABRIEL T.:14471:720:Npt_BR
sigepi.autor.atividadeRODRIGUES, VANESSA G.:11690:720:Npt_BR
sigepi.autor.atividadeLEME, DANIEL R.:14114:720:Npt_BR
sigepi.autor.atividadeYAMAGATA, CHIEKO:177:720:Spt_BR
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