Bioactive composites containing TEGDMA-functionalized calcium phosphate particles: Degree of conversion, fracture strengthand ion release evaluation
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ANA HELENA DE ALMEIDA BRESSIANI
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Dental Materials
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Objective. To evaluate the strength and ion release of experimental composites containingTEGDMA-functionalized calcium phosphate particles.Methods. Seven composites containing equal parts (in mols) of BisGMA and TEGDMA and60 vol% of fillers were manipulated. Filler phase was constituted by silanized barium glassand 0% (control), 10% or 20% (volume) of dicalcium phosphate dihydrate (DPCD) particles,either non-functionalized or functionalized with two different TEDGMA contents. DCPDparticles were synthesized and characterized by X-ray diffraction (XRD), elemental analysis,surface area and dynamic light scattering. Composites were tested for degree of conversion(DC) by near-FTIR. Biaxial flexural strength (BFS) was determined after 24 h and 28 days inwater. Calcium and phosphate release after 7 days was assessed using inductively coupledplasma optical emission spectrometry (ICP-OES). Data were analyzed by ANOVA/Tukey test(alpha:5%).Results. XRD confirmed the crystalline structure corresponding to DCPD. Elemental analysisrevealed particles with zero, 14% or 22% TEGDMA, with similar D50(around 19 m) andsurface areas from 3.5 to 11.4 m2/g. The presence of DCPD did not reduce DC. After 24 h,functionalization (both 14% and 22% TEGDMA) improved composite strength in comparisonto non-functionalized DCPD, both at 10% and 20% levels. After 28 days, BFS of materialscontaining 10% functionalized DCPD were statistically similar to the control containing onlybarium glass. Among composites containing 10% DCPD, particle functionalization with 14%TEGDMA did not jeopardize ion release.
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ALANIA, YVETTE; CHIARI, MARINA D.S.; RODRIGUES, MARCELA C.; ARANA-CHAVEZ, VICTOR E.; BRESSIANI, ANA H.A.; VICHI, FLAVIO M.; BRAGA, ROBERTO R. Bioactive composites containing TEGDMA-functionalized calcium phosphate particles: Degree of conversion, fracture strengthand ion release evaluation. Dental Materials, v. 32, p. e374-e381, 2016. DOI: 10.1016/j.dental.2016.09.021. Disponível em: http://repositorio.ipen.br/handle/123456789/26918. Acesso em: 10 Jun 2026.
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