Method development and validation for simultaneous determination of IEA-R1 reactor’s pool water uranium and silicon content by ICP OES

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dc.contributor.authorULRICH, J.C.
dc.contributor.authorGUILHEN, S.N.
dc.contributor.authorCOTRIM, M.E.B.
dc.contributor.authorPIRES, M.A.F.
dc.coverageInternacionalpt_BR
dc.date.accessioned2018-08-02T16:53:05Z
dc.date.available2018-08-02T16:53:05Z
dc.date.issued2018pt_BR
dc.description.abstractIPEN’s research reactor, IEA-R1, an open pool type research reactor moderated and cooled by light water. High quality water is a key factor in preventing the corrosion of the spent fuel stored in the pool. Leaching of radionuclides from the corroded fuel cladding may be prevented by an efficient water treatment and purification system. However, as a safety management policy, IPEN has adopted a water chemistry control which periodically monitors the levels of uranium (U) and silicon (Si) in the pool’s reactor, since IEA-R1 employs U3Si2-Al dispersion fuel. An analytical method was developed and validated for the determination of uranium and silicon by ICP OES. This work describes the validation process, in a context of quality assurance, including the parameters selectivity, linearity, quantification limit, precision and recovery.pt_BR
dc.format.extent1-5pt_BR
dc.identifier.citationULRICH, J.C.; GUILHEN, S.N.; COTRIM, M.E.B.; PIRES, M.A.F. Method development and validation for simultaneous determination of IEA-R1 reactor’s pool water uranium and silicon content by ICP OES. <b>Journal of Physics: Conference Series</b>, v. 975, n. 012012, p. 1-5, 2018. DOI: <a href="https://dx.doi.org/10.1088/1742-6596/975/1/012012">10.1088/1742-6596/975/1/012012</a>. Disponível em: http://repositorio.ipen.br/handle/123456789/29013.
dc.identifier.doi10.1088/1742-6596/975/1/012012pt_BR
dc.identifier.fasciculo012012pt_BR
dc.identifier.issn1742-6588pt_BR
dc.identifier.orcidhttps://orcid.org/0000-0002-6462-4758
dc.identifier.orcidhttps://orcid.org/0000-0003-2604-1225
dc.identifier.percentilfiSem Percentilen
dc.identifier.percentilfiCiteScore16.00
dc.identifier.urihttp://repositorio.ipen.br/handle/123456789/29013
dc.identifier.vol975pt_BR
dc.relation.ispartofJournal of Physics: Conference Seriespt_BR
dc.rightsopenAccesspt_BR
dc.subjectvalidation
dc.subjectpool type reactors
dc.subjecturanium
dc.subjectsilicon
dc.subjectemission spectroscopy
dc.subjectoptical systems
dc.subjectplasma
dc.titleMethod development and validation for simultaneous determination of IEA-R1 reactor’s pool water uranium and silicon content by ICP OESpt_BR
dc.typeArtigo de periódicopt_BR
dspace.entity.typePublication
ipen.autorMARIA APARECIDA FAUSTINO PIRES
ipen.autorMARYCEL ELENA BARBOZA COTRIM
ipen.autorSABINE NEUSATZ GUILHEN
ipen.autorJOAO CRISTIANO ULRICH
ipen.codigoautor1327
ipen.codigoautor515
ipen.codigoautor5931
ipen.codigoautor632
ipen.contributor.ipenauthorMARIA APARECIDA FAUSTINO PIRES
ipen.contributor.ipenauthorMARYCEL ELENA BARBOZA COTRIM
ipen.contributor.ipenauthorSABINE NEUSATZ GUILHEN
ipen.contributor.ipenauthorJOAO CRISTIANO ULRICH
ipen.date.recebimento18-08pt_BR
ipen.identifier.fiSem F.I.pt_BR
ipen.identifier.fiCiteScore0.7
ipen.identifier.ipendoc24803pt_BR
ipen.type.genreArtigo
relation.isAuthorOfPublication2254b498-a2dd-4f3f-a64d-d0d6e8a3acdf
relation.isAuthorOfPublicationcc013e19-0c8e-4f8c-845f-f2ff7471b78a
relation.isAuthorOfPublicationc3932232-0001-4122-bc0e-9109d11f8bec
relation.isAuthorOfPublicatione6eb5864-afb7-42d6-8897-2afbf3d944d8
relation.isAuthorOfPublication.latestForDiscoverye6eb5864-afb7-42d6-8897-2afbf3d944d8
sigepi.autor.atividadeULRICH, J.C.:632:510:Spt_BR
sigepi.autor.atividadeCOTRIM, M.E.B.:515:510:Npt_BR
sigepi.autor.atividadePIRES, M.A.F.:1327:510:Npt_BR
sigepi.autor.atividadeGUILHEN, S.N.:5931:510:N
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