The influence of crucible material on the DSC thermal analysis compared to freeze-drying microscopy results

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dc.contributor.authorTATTINI JUNIOR, VIRGILIOpt_BR
dc.contributor.authorPARRA, DUCLERC F.pt_BR
dc.contributor.authorPITOMBO, RONALDO N. de M.pt_BR
dc.coverageInternacionalpt_BR
dc.date.accessioned2014-07-15T13:41:36Zpt_BR
dc.date.accessioned2014-07-30T11:51:32Z
dc.date.available2014-07-15T13:41:36Zpt_BR
dc.date.available2014-07-30T11:51:32Z
dc.date.issued2009pt_BR
dc.description.abstractThe aim of this study was to investigate the influence of different crucible materials on the thermal analysis of binary systems. The thermal properties of two distinct solutions were measured both by Differential Scanning Calorimetry (DSC) and freeze-drying microscopy and the results were compared. The glass transition of the maximally freeze-concentrate (Tg′) and the eutectic melting temperature (Teut) were not influenced by the crucible material. However the heat of fusion (ΔH) involved during the Teut as well as the ΔC p involved during the T g′ of the solutions were affected.
dc.format.extent203-206pt_BR
dc.identifier.citationTATTINI JUNIOR, VIRGILIO; PARRA, DUCLERC F.; PITOMBO, RONALDO N. de M. The influence of crucible material on the DSC thermal analysis compared to freeze-drying microscopy results. <b>Journal of Thermal Analysis and Calorimetry</b>, v. 98, n. 1, p. 203-206, 2009. DOI: <a href="https://dx.doi.org/10.1007/s10973-009-0317-8">10.1007/s10973-009-0317-8</a>. Disponível em: http://repositorio.ipen.br/handle/123456789/4856.
dc.identifier.doi10.1007/s10973-009-0317-8
dc.identifier.fasciculo1pt_BR
dc.identifier.issn1388-6150pt_BR
dc.identifier.orcidhttps://orcid.org/0000-0002-7626-880X
dc.identifier.urihttp://repositorio.ipen.br/handle/123456789/4856pt_BR
dc.identifier.vol98pt_BR
dc.relation.ispartofJournal of Thermal Analysis and Calorimetrypt_BR
dc.rightsopenAccessen
dc.subjectlyophilizationpt_BR
dc.subjectcruciblespt_BR
dc.subjectthermal analysispt_BR
dc.subjecttransition temperaturept_BR
dc.subjectmicroscopypt_BR
dc.subjectcalorimetrypt_BR
dc.titleThe influence of crucible material on the DSC thermal analysis compared to freeze-drying microscopy resultspt_BR
dc.typeArtigo de periódicopt_BR
dspace.entity.typePublication
ipen.autorDUCLERC FERNANDES PARRA
ipen.codigoautor562
ipen.contributor.ipenauthorDUCLERC FERNANDES PARRA
ipen.date.recebimento09-12pt_BR
ipen.identifier.fi1.587pt_BR
ipen.identifier.ipendoc14260pt_BR
ipen.identifier.iwosWoSpt_BR
ipen.range.fi1.500 - 2.999
ipen.type.genreArtigo
relation.isAuthorOfPublication67996d86-0a59-4ba2-8d38-facaa14e26c3
relation.isAuthorOfPublication.latestForDiscovery67996d86-0a59-4ba2-8d38-facaa14e26c3
sigepi.autor.atividadePARRA, DUCLERC F.:562:740:Npt_BR

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