Determination of the crystallographic texture of sintered PrFeB magnets based on X-ray diffraction patterns

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Journal of Magnetism and Magnetic Materials
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An alternative method for determining the degree of crystallographic alignment (〈cos Θ〉) of the magnetic Pr2Fe14B phase (Φ) is proposed. The method is based on the relative X-ray diffracted intensities of the Φ planes of sintered magnets with and without texture. The degree of crystallographic alignment is also determined by X-ray pole figures using the (0 0 4) reflection and considered as a standard reference for comparison. The method is applied to Pr16Fe76B8 magnets with 0.51≤〈cos Θ〉≤0.97. The difference between the crystallographic alignments determined by these two methods is 3% within the experimental error. The advantages and limitations of using X-ray diffraction patterns to quantitatively evaluate the texture of sintered magnets are also discussed.

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PERIGO, E.A.; TAKIISHI, H.; MOTTA, C.C.; FARIA, R.N.; LIMA, N.B. Determination of the crystallographic texture of sintered PrFeB magnets based on X-ray diffraction patterns. Journal of Magnetism and Magnetic Materials, v. 320, n. 14, p. e40-e42, 2008. DOI: 10.1016/j.jmmm.2008.02.012. Disponível em: http://repositorio.ipen.br/handle/123456789/4944. Acesso em: 20 Mar 2026.
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