Low-temperature reduction of graphene oxide using the HDDR process for electrochemical supercapacitor applications
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2018
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CONGRESSO BRASILEIRO DE ENGENHARIA E CIÊNCIA DOS MATERIAIS, 23.
Resumo
In the present work, attempts of reducing a graphene oxide powder using a low
temperature hydrogenation disproportionation desorption and recombination process
(L-HDDR) has been carried out. A lower processing temperature in large scale
production is significant as far as costs are concerned. Graphite oxide was prepared
using a modified Hummers’ method and dispersed in ethanol, exfoliated using
ultrasonication to produce Graphene Oxide (GO). Investigations have been carried out
by X-ray diffraction (XRD) and scanning electron microscopy (SEM). The experimental
results of L-HDDR processing graphene oxide powder using unmixed hydrogen at
400°C and relatively low pressures (<2 bars) have been reported. X-ray diffraction
patterns showed a reduction of graphene oxide with the L-HDDR process. The results
showed that the L-HDDR process, as the standard HDDR process, can be applied to
the reduction of graphene oxide to produce supercapacitor materials. The advantage
of employing the L-HDDR process is a relatively a low temperature would reduce the
cost of treatment that is a very important factor for producing large amount of material.
Thus, the L-HDDR process has been considered a promising alternative method of
reducing graphene oxide with efficiency and possibly in large scale production.
Como referenciar
BENITEZ JARA, F.G.; CRUZ, P.V.; BARBOSA, L.P.; CASINI, J.C.S.; PERUZZI, A.J.; SAKATA, S.K.; FARIA, R.N. Low-temperature reduction of graphene oxide using the HDDR process for electrochemical supercapacitor applications. In: CONGRESSO BRASILEIRO DE ENGENHARIA E CIÊNCIA DOS MATERIAIS, 23., 04-08 de novembro, 2018, Foz do Iguaçu, PR. Resumo... p. 2922-2922. Disponível em: http://repositorio.ipen.br/handle/123456789/29627. Acesso em: 20 Mar 2026.
Esta referência é gerada automaticamente de acordo com as normas do estilo IPEN/SP (ABNT NBR 6023) e recomenda-se uma verificação final e ajustes caso necessário.